免费文献传递   相关文献

Determination of atranol, lecanorin, ethyl orsellinate and methyl orsellinate in Usnea diffracta by RP-HPLC

RP-HPLC同时测定高挂草中4种酚酸类成分的含量



全 文 :38;.8B
Z7%ԗ˜{r
^
 ™@¨
Ú6[Z·
®¯°
#
\|
#
±²f
!
!
8;I¯J nVe¯3kLMN 8IJQýlm#34Æe¯ÿ89:; no7
šEK3ÿ89:;
#
no nV
[OMMMM
$
†;
%!

&
stZ7%ԗ˜{r
$2%$)/&!
P½@
!
ã{@
!
ã{@ُZ·[¢j—éžj{‰”

ˆ‰
.
C%/I$0&
PN
{‰Œ
$^hX IIkWLM II! L
!
I%&

Pg
†™@ê&Êj
=!
ê&Êj
7!
²³´
&
1%µxê
WNM )I&
&L
PhM IB/ I)
QP
&
Ψ
WL j
Š‹
. =2%$)/&!
P½@
!
ã{@
!
ã{@ُ]%Ô2Û~Œ¼RKI>[n›
&
¹ŒÈH‹
6Fê
PMPh_g!_XhOg!_LhOg!PMWh_g!31R
6Fê
WhOg!Ph_g!Ph_g!Ph_g
ŠŒ
.
¤…”ãEyH
#
6m
#
iR›>
#
+/‹—
!
*›Z7%Ô|ù;{Ǘ˜{r
$2%$)/&!
P½@
!
ã{@
!
ã{@ُ[Z·

$
Ž
%!
—˜{
&
|ù;
&$2%$)/&&
P½@
&
ã{@
&
ã{@ُ
$
8$f
%!WMPMPPPLMPW
$
‘ ’ E q
% !
r ­ ö ] b
)
) Ø g I
*
±   õ P u v
$M_M^WX+d?P%&
µäRléö]stuv
$M[PM39d=PWM%&
µäR
Rrˆ÷ö÷st.Cuv
$M__39c=MM_%
$
“„>”
%!
!
™¹
! @(&.$M_OP% ^_XNWMN! -;I$&. )UG&0#&GUhG$0hG) /%0#AU\&GUhG$0hG)
!!
—˜{
$
|ùÇM
.
|yJåæS
%
ê|ù;±
N›{Çg|
!
AÑÒ¿ ¨â[‰ÿ˜¸Gç
öxЅTwè÷>[Òé

ËLM[Ǭ¨C
R|ù;±}Jö}JKÉ̀.}J
%43,.
?0=/.*!. S$)h
E—˜{ÐÇ
P(

¤2DÙؾA
—˜{8É>Fã[\]Ú6GY›ƒ„
W;^(
!
—˜
{r‚&Zè™@
#
¢™@G¢™@*`¨Ú6
!
>
Ƨªwè–>[?NY›

ê8|M—¬›|
ù;Ï;Ǜ™¬
!
¤7p5st>
.8B
Z7%
ԗ˜{r
^
 ™@›Ú6
$$2%$)/&!
P½@
!
ã{
@
!
ã{@ُ
%
Z·[…”

!
ÁÂ
=*&()2PPMM
â—éžj{‰ß
!,S;PMMR=R
1%à
$=*&()2!,1=% =2%$)/&!
P½@
!
ã{@

!
ã{@ُ
^
 A“]x¤§¨ylÜ
W;^(
ª
P
.;><3!
PO
;><3
Ñ
<1
()i7«1#
L;N(
[
$2%$)/&!
P½@
!
ã{@
!
ã{@ُj|A
!
l
Ë
.8B

!
Œu
_Ng
†™@
#
Œê
6‹l
!
l8e\]çÛüå
!
rsm
$
èéél
om
%
—˜{ÇÁÐ
O
Ã
!
6F“lµäRäý
|ù;lÑT
!
Ëý…Ïöu]4êäöÕÔê}
Jö}JKÉ̀.}J
%[?0=/.*!.
[O{
!
ÉÆ
À¤
$>/hWMMLMM[ lWMMLMM_%
Œtröb)ø¯
{É̙¬\]i-§¨y

#
…”i0•
#]!
{‰;q
!
{‰Œê
C%/I$0&
PN
$^hX IIk
WLM II!L
!
I%
{‰Œ
!

Pg
†™@ê&Êj
=!
ê&Êj
7
8ɲ³´
!M lL I)![Mg =&
L lPL I)!LMg =&
&L
PhM IB/I)
QP
&
Ψ
WL
j&
1%µx
WNM )I&
8ƒ·ê
WM
!
B
]_£{‰
;qª
!
{º–>64
!
{‰dŸd
P
Ph=2%$)/&&Wh
P½@
&Oh
ã{@
&^h
ã{@ُ

d
P!
A“]ž
$=%
i—˜{
$7%.8B
d
#]#
A“]ž[ÜÝ
!
93P#
$2%$)/&$P%!
P
½@
$W%!
ã{@
$O%!
ã{@ُ
$^%
A“]Á
·
!
َQ>Ô
!
ÜÚ
P */B
QP
[¿A“]Ã
ݞ

/OOWW/
{
OX
ï{
PX
•
WMPP
÷
N
²
!!!!!! ! ! ! ! ! !!!! ! ! ! !
S/&hOX! :004(!PX
=4*402! WMPP
#]$
oç]ž[ÜÝ
!
#ƒ]†‡~
MhL *$^

%!
93PÔ
!
œë;Y€r
!
aÐَ
WL IB!
XM j
È&
!
µ#
W
5
!
75
OM I)!
Ä>
W
5َµ

!
rǝÛ
!
áâ›ÙŽ ÙQ
!
ԝ
PM
IB
·€
!
›
Mh^L
!
I
±¡°
!
ݛ

#]%
n›‰F‘ú
!
6F#A“]Ãݞ
!
›Ù
ŽsÚ
P!W!L!WM!WL!PWL
ý
!

X
Y·<
²[À+ž
!
¦5G#
WM
!
B

!
]
WNM
)I
Ö1%
!
8ƒ<
$E%
ꅄ!
{TU
$D%
ꃄ!
&È9….
#
j‰F(Gn›2
Û
!
0•Ÿ¼
P
¼
P!
A“]
P l^
[n›‰F
$3YX%
A“] A-7š
ZI)
È9…. H
W
P Nh_PL DYPPP W^OEQPXhPNW Mh___ X
W PMhL_ DY^ [ NPNEQXhNXW P Mh___ _
O POhPW DYWN LLXEQPWh[LN Mh___ N
^ POhXW DYLM [PXEnLhO^O L Mh___ _
!!
?
.
n›2Û
PhX lWMM I*/B
QP

#]&
93ç¨
!
93G#Z|A“]ž
WM
!
B!
E¼ij8ƒ
X
5
!
¥%{TU
!
.P&
$2;
%$)/&!
P½@
!
ã{@
!
ã{@ُ
^
 A“]
{TU[
31R
6Fê
PhPg!PhPg!Ph_g!Ph^g
#]
zԛç¨
!
93G#Z|oç]ž
!
y
®ª6FÉܾ
M!^!N!PW #
8ƒ6‹
!

$2;
%$)/&!
P½@
!
ã{@
!
ã{@ُ
^
 A“]
{TUU6_


31R
ê
PhOg lPhNg!
¼.o
ç]ž]
PW #
~s¤zÔ

#](
ij›ç¨
!
6FP#Z|Ã]Ð
X
7
!
7
7~
MhL *!
93PÔ
!
ÜÝoç]ž
!
¦”%Ô
$2%$)/&#
P½@
#
ã{@Ñã{@ُ[¹ŒY
·6(6Fê
MhMPPg! MhMM[ Lg! MhMM[ Ng!
MhWPg!31R
6Fê
Ph[g!PhNg!PhXg!PhOg!
ƒ
]ij›I>

#])
aƒÈH‹ç¨
!
#ƒ]~
MhL *!
Ð
X
7
!
9
3PÔ
!
6F93aÐ
$2%$)/&!
P½@
!
ã{@
!
ã{@ُ
^
 A“]ž
$
Y·<6Fê
OOhO!NXhL!^^h^!N_hP I*/B
QP
% W IB!
ÜÝoç]
ž
!
8ƒ%Ô
!
.PÈH‹
!
Ÿ¼
W!

$2%$)/&!
P½@
!
ã{@
!
ã{@ُ[¹ŒÈH‹Ñ
31R
6 F ê
PMPh_g! WhOg& _XhOPg! Ph_g&
_LhOMg!Ph_g&PMWh_g!Ph_g
¼
W!^
 ™@¨Ú6aƒÈH‹
$3YX%
Ú6
ƒ]r·
ZI*
aз
ZI*
%&·
ZI*
ÈH‹
Zg
¹ŒÈ

Zg
31R
Zg
=2%$)/& MhMLX N MhMXX X MhPWO O __hN PMPh_ WhO
MhMLX L MhPW^ L PMWhP
MhMLX M MhPWO N PMPhN
MhMLX L MhPW[ M PMLhN
MhMLX W MhPWW W __hP
MhMLX [ MhPWL M PMWhL
P½@
MhMO[ X MhP[O M MhWMO M _LhX _XhO Ph_
MhMO[ W MhWMW M _LhO
MhMON W MhWMP M _^hP
MhMON M MhWM^ M _Lh_
MhMO[ ^ MhWM_ M __hW
MhMO[ N MhWM[ M _[hN
ã{@
MhMON ^ MhMNN N MhPWP M _OhM _LhO Ph_
MhMON P MhPWO M _LhX
MhMON [ MhPWW P _Oh_
MhMON L MhPWW X _^h[
MhMON X MhPW^ W _Xh^
MhMON M MhPW^ _ _[h_
ã{@ُ
PhMWO X MhP[N W PhWMW M PMMhP PMWh_ Ph_
PhMWO P PhWP PM^h_
PhMWO O PhWP PM^hN
PhMWO L PhWM^ PMPhO
PhMWO O PhWMN PMOhX
PhMWO ^ PhWMX PMWhL
#]*
ƒ]%Ô
!
’“
#]$
u²£…”8É
O
Ó
lµäRäýT[|ù;{Ǘ˜{ƒ]žÜ
Ý
!

#]!
{‰;q8ÉZ·%Ô
!
Ÿ¼
O
¼
O!
µäRäý|ù;lÑT“H[—˜{
r
^
 ™@¨Ú6
$3YO%
!
*/*
QP
ƒ]Wf
$2%$)/&
P½@ ã{@ ã{@ُ
WMMLMM[ PPWhL [Mh_ [Lh[ P__hW
WMMLMMN PPOhX [LhW [[hX WM^hX
WMMLMM_ PPMhW [WhP [XhW P_NhX
$
†,
$]!
1%µx[´µ
!
6FA
$2%$)/&!
P½@
!
ã
{@
!
ã{@ُ
^
 A“][َž8
É>¡®¬­
!
&b
$2%$)/&!
P½@
!
ã{@

!
ã{@ُ[¸uGHµx¦5ê
WNM!
W[M!WXL!WXL )I

R=R
1%à
!
6F]_
£
^
µxªAƒ]8É>1%

0•¼.
!
]
/^OWW/
{
OX
ï{
PX
•
WMPP
÷
N
²
!!!!!! ! ! ! ! ! !!!! ! ! ! !
S/&hOX! :004(!PX
=4*402! WMPP
W[M
Ñ
WXL )I
ª%Ô7
! $2%$)/&
[{‰{[{
TU.u6
!
f]
WNM )I
ª
!
¿{‰{64I
>
!
sn¹z
!
<«%
^
 Ú6[{TUì|”
!
¸/Ô1%µxê
WNM )I
$]#
µ#;q[´µ
!
«%
^
 Ú6[Z·ê

!
‘4b
$2%$)/&!
P½@
!
ã{@
!
ã{@Ù
]َrQ›>
!
Z7‘4baP謝«%
ÌYK
!
@½¸/Ô>َ
WL IB!XM j

&
!
µ#
W
5
!
75
OM I)
[µ#…”

$]$
&Êj[´µ
!

^
 «%[\Ä̌K
™@¨Ú6
!
²&Êj[
U.
äAB{âGA
-7š
!
Î͛
Pg
†™@
;
ê&Êj7
!
$2%$)/&!
P½@
!
ã{@
!
ã{@ُ’kb>
÷>[64

%
0,
¤§¨“›—éžj{‰”p5AµäR|ù
;{Ǘ˜{r[
^
 ™@›Ú68É>Ô·6
‹

§¨m¡A{‰;q[7!
Í¿\ÄÌkb
>I>[64
!
÷…”y¾
#
6m
#
+/›—

­®
!
$2%$)/&!
P½@
!
ã{@
!
ã{@ُ—
^
 ™
@›Ú6ꗘ{?NY›ØI[ÙÚÚ6
W(
!
+
/%ÔªZ·V謝8|M—æA—|¯{Ï;
ÇÌ[—¬›ƒ„

$
•ƒ–—
%
P(!
¦ì
!
Ûku
h
r­e(Ï;!ãÏÇuF
<(h
5{
.

íö]÷ÑKÂÐ
! WMMM.POOMh
W(!
îï±
!
™¹
!
ð8Ÿ
h
—˜{µ#Ì[Ü݅”
.

!
>PMP^XPNWN8(hWMM_;MX;W^h
O(!e.4$)A$)*! 9) c4$)U()*! 1#c$)U)*F=)(E5(U05/)(6%/I
%43,. ?0=/.*!. 9(h#) #(IB(2! WMM_! WM$W%. PN[h
^(!
îï±
h
|ù;ÇÌ\]Ú6GãÌY›ƒ„
R(h
ïG
.
r
­ö]bïG\]Ì¥ƒ„²
!WMMNh
L(!c$)*+9! a() 45 6(%I()2)$U%/54G206%/I2#()!/,C!<@A*,4c:<;O^PWP 9(h
>$28%/5 3(0R(D! WMMX! PN. [Xh
X(!
>­.
!
CñI
!
ò­k
!
‡
h
énóŸ.R[\]Ú6
9(h
!ýÉ̃„
! P__M! PW. ^L[h
[(!CHI$.! :5(@! T204V$.! (2$&ha$2(%;0/&4b&(U#()/&G*&AG/;
05(06%/I&($D(0/6#-.3:0+@C/,@30=<-0+@9(h8#A2/G#(I02%A!
P__[! ^^. PLLPh
N(!

!
ír7
!
4øã
h
\ó¸}[\]Ú6
9(h
!ýÉÌ
ƒ„
! P__M! PW$^%. ^^[h
@ADAG.0C/D0BCBM/DG/CB1! 1AU/CBG0C! ADEF1BGKA10C/DA/CH.ADEF1
BGKA10C/DA0C=,+% 5)7($ OF :P-3P;2
e:.4$)A$)*! .->94$)! 1.:c$)U)*
!
$L,A$.1,@04!/A<=NU,4!,/3 -.3!H,4<+/*,4]N.!+/.-8,?0*03,<=.34+
/<+ ;34!0!+!,<=6>,@0*.->A40*4! 6>03,4,#*.?,@A<=)*0,3*,4! $.3M><+ [OMMMM! 6>03.%
6OKDG/UD(8O[AUD0SA. @/5(D(&/U $38;.8BI(2#/5 6/%5(2(%I))*2#(G/)2()20/6$2%$)/&! &(G$)/%)! (2#A&/%0(&)$2($)5
I(2#A&/%0(&)$2() %43,. ?0=/.*!.h>ADEBH. =C%/I$0&;
PN
G/&4I) $^hX IIkWLM II! L
!
I% E$040(5 $2WL j E2# 2#(I/b&(
U#$0(0/6$G(2/)2%&(;Pg $G(2G$G5 ) $*%$5()2I$))(%h@#(6&/E%$2(E$00(2$2PhM IB/I)
QP
h@#(5(2(G2/) E$D(&()*2# E$0
WNM )Ih:AKI1D. @#(G/%(&$2/) G/(6G()20/6$2%$)/&! &(G$)/%)! (2#A&/%0(&)$2(! $)5 I(2#A&/%0(&)$2(E(%(#*#(%2#$) Mh___h
3(G/D(%(0E(%(6%/IPMWh_g 2/_LhOMg& E2# 31R6%/IWhOg 2/Ph_gh2BCU1IK0BC. @#(I(2#/5 0]4GV! 0IU&($)5 %(U($2$b&(
6/%0I4&2$)(/405(2(%I)$2/) /6$2%$)/&! &(G$)/%)! (2#A&/%0(&)$2($)5 I(2#A&/%0(&)$2() %h?0=/.*!.h
A^F WBGHK(!%43,. ?0=/.*!.& c4*4 )$2/)$&2A& $2%$)/&& &(G$)/%)& (2#A&/%0(&)$2(& I(2#A&/%0(&)$2(
HB0.!+_%#)RU[U..#+!!!!)
$
˜™$Q
!
¦Z§
%
/LOWW/
{
OX
ï{
PX
•
WMPP
÷
N
²
!!!!!! ! ! ! ! ! !!!! ! ! ! !
S/&hOX! :004(!PX
=4*402! WMPP