免费文献传递   相关文献

UPLC characteristic chromatographic profile of Paeoniae Radix Alba

白芍药材UPLC特征指纹图谱研究



全 文 :vbÇÁ
,8C
±yzfQƒ„
EL
R
#
.65
X
#

X
#
EL
R
#

Q
#
RST
Q
#
–š
R
!
!R:
“$HF>¬ 5H¬G
#
*Ý “$
RRMMRY%
X:
™Zœ[HKLMNOPQ
#
™Z C©õ
XXXMMR%
Q:
“$HF>¬ H¬G
#
*Ý “$
RRMMRY
$
”;
%!

&
BCvbÇÁ[
,8C
±yzfQ6…©
!
êRNADvbÇÁ[[·
!
Ÿìvb[[·@܅©
µq¥)

–—
,
ғ
>e,;Ac,8C.11 AQ
}QÚ
$XfR IIgRMM II!RfN
!
I%!
=ÊjŠ.
ÄB_ÏJ
!
”&Ûz
XQM )I
˜™
,
BC‰vbÇÁ[
,8C
±yzfQÐèXš
!
Àԉ
RL
ÐèÈ
!
)‰ªr
L
ÐèÈ
!RL
ÃvbÇÁ
[j!(ê
MfN`R mMf``Y
˜š
,
à…©RN
!
*“•ADvbÇÁ[·

$
›œ
%!
vb
&
±yzfQ
&,8C
$
8…$f
%!XMRRMXRRMM$
†‡Eq
%!
­æ
.
k£‹Ç=Ü
/
øùk£­u
$XMM`d+M`QMN<
MMQ!XMM`d+M`LM_$
ˆ€>‰
%!
!
Ž
!
F‚‰
!
ߨãÀÄ
!
‚&³ÙrÇÇéÌ[
s¨i[·@܃„
!-!!
vbêuøÉÌbÇ
2#<.,%# =#!%&=.+# 8$&f
[6/ì

ªèO
#
B
!
Z^

#
Í

yèŒ
S9Í
!
#àÿ$
!
%Kÿö
!
—‰Kágàé

“
•S]&¨
!
´ÍY9
!
n$
!
$
!

!

!
˜S

!
†ö*+
R(

vh
!
‘Ò“bÇw)H|Ú
6Eêvb[[·@ÜÀ
!
­OV@Üvb[
~][·
!
>Cª*,“-³KŸ‘


.8C
…©BCÇÁ[zfQ
!
>Xj!(6ùӓ•ÇÁ[zfQÑè7«4ø
X!
ìғ
,8C
BCvbÇÁ[zfQ6…©­~œ|
Ê4ø

Ÿ¡éJj}Q
$,8C%
ä
RfN
!
I
[ŸK
}QÚÞÂê+áùÓ[‹â}Q6ˆ6ùÓ
!
jC•ÉÓ
.8C

!,8C
èüß[6ˆé[G
vO(
_
£ç§p5ғ
,8C
©BCvbÇ
Á[±yzfQ6…©
!
ªQÈ[Aâ9’O
Ø]
` I)
~
!
J£Q¤f69’
!
µ¡6é
[
!
ê¡é
#
RNQADvbÇÁ[·µq…©

!
ÁÂ
>e,;Ac,8C$

b$2(%0
˜
!
wx˜;¡
O;()
#
*ev(¼
#
nÊî®à
#
Ú¤3
#
ýJ*
*J”&à
#-IV/F(%X
}QNE»
%!78XRM1


$

1$%2/%40
˜
%!>7RQL<1 R[RM
m:—
$=-AAC-3AOC-TO
ßàè&˜
%
C2>öJ“B
#
.Çû
#
vbw
#
bÇw
#
­”
‹bÇwŒênÜ
$
Í+/Ñ[QÕÔ
!
ғÈV
W<|^©/R
!
O(Œ£•
`Nh%&
Š.
#
”•
#
Ä
Bê}QO
!
Š•ê6O
!
_êKLLO‚_
&
v
bÇÁÍWáÇø£_rÇ_ûŽF‚‰ÕÔê
»>
!
3ÓAŽ•àþ6/Ö
!
ª;¬Ê¼
R
¼
R!
vbÇÁ®>[;¬
?/:
ÇÁ;¬ ±yzfQWf
R
é 0-
R 1R
X
é ÖÑ
R 1X
Q
é 0-Ú÷ã
1Q
_
é 0-„÷ã
1_
L
é 0-ý÷ã
1L
Y
Ç! ¤T
1Y
ôÈ ïð
1N
©þ 1
1N
`
é 2˜
1`
RM
é ÖÑ
X 1RM
RR
é 0-
X 1RR
RX
é 0-
Q 1RX
RQ
é 0-
_ 1RQ
R_
é 0-
L 1R_
RL
é 0-
Y 1RL
#
…©i0Œ
# !^
}Qâs
>e,;Ac,8C.11 AQ
}QÚ
$XfR IIgRMM
-XR\-
{
QY
ï{
Y
—
XMRR
÷
Q
´
!!!!!! ! ! ! ! ! !!!! ! ! ! !
U/&fQY! ;004(!Y
=$%G#! XMRR
II! RfN
!
I%&
=ÊjŠ.
$>%ÄB_ÏJ
$7%
;(ýv
,M mMfL I)!\h mR_h>&MfL mXfL
I)!R_h >&XfL mQ I)!R_h mXMh>&Q mY I)!
XMh mXXh>&Y mYfL I)!XXh m_Mh>&YfL mN
I)!_Mh mLMh>&
;(ƒpŒê›p

=N
MfL
IC-I)
&
”&Ûz
XQM )I&
Ú¤
QM l&
î®
·
R
!
C
# #^
C2>ÏJ[ÜÝ
$öJ“B
#
.Çû
#
vbw
#
bÇw
#
­”‹b
ÇwC2>Å·
!
93PÔ
!
“”•ÐÜÚ\öJ“
B
#
.Çû
#
vbw
#
bÇw
#
­”‹bÇw[·>(
6Ñê
MfRRX L!MfMQ\ LM!Mf_Q_ \!RfRX\!MfMQM RL
*-C
SR
[ÔÄC2>ÏJ
!
B]ݓ

# $^
qç>ÏJ[ÜÝ
$®>VoB
MfL *!
93PÔ
!
%
RM IC
·C
r
!
a
LMh
Š•
N IC!
ŸÛÖ¤
QM I)!
_:ܤ
!
a
LMh
Š•:Ù(
!
64
!MfXX
!
I
ZB‡ù‡ 
!
$чJ
!
Õ

# %^
…©_“Ä
# %^ !^
93(ç§
!
$Z|qç>ÏJ
!
—
# !^
u¬…©‰Ñî®
Y
5
!
&ª¿ÐèÈjCAâ
9’ÑjCÈVW[
31T
Œ8•
QfMh!
¼.93
(žß

# %^ #^
klç§
!
$Z|î>
Y

!
—
# $^
u
¬ÝEÜÝqç>ÏJ
!
—
# !^
u¬…©6Ñî®
!
&ª¿ÐèÈjCAâ9’
#
jCÈVW[
31T
Œ8•
QfMh!
¼.klžß

# %^ $^
dԝç§
!
$Z|qç>ÏJ
!
—
# !^
u¬…©6Ñ]
M!X!_!Y!N!RX!X_ #
î®&Ô
!
ª
¿ÐèÈjCAâ9’
#
jCÈVW[
31T
Œ8•
QfMh!
¼.®>ÏJ]
X_ #
~dÔ

# &^
®>&Ô
$
RL
ÃvbÇÁ®>
!
—
# $^
u¬…©ÜÝq
ç>ÏJ
!
]
# !^
u¬[}Qâs¬¥5&
!
ˆ%}Qf
!
ÐÀ
RL
ÐèÈ
!
)ªr
L
Ð
èÈ
!
6ÑêöJ“B
$Q

%#
.Çû
$L

%#
vbw
$Y

%#
bÇw
$fÈ
%
Ñ­”‹bÇw
$R_

%
ÒâvbÇÁ}QfÊf
R
# ^
±yzfQ[BC
# ^ !^
’ƒÈ[¶·
!
]¿Ã5®>fQrbÇ
w[}QÈ
$Y

%
6ˆžß
!
ÈI3r
!
ÈVW„
£nê²è®>Ðè
!
²/ÔbÇwê’2È

f
R!
vbÇÁ[
,8C
f
# ^ #^
±yzfQ[BCGj!(AD
!
X
²[
RL
ÃvbÇÁ
,8C
fQ
>;>
Ś¥
5ÀÒ
*
rÇ}QzfQj!(ADHå
XMM`
Ä
+
fs
!

1R
ÃÇÁQfEê’2Qî
Ëz¼Ð
!
/ԉ
RL
ÐèÈ
!
BC‰ÐèX
šÊf
X!
>îˉj!(/R
!RL
î>[j
!(ʼ
X
f
X!RL
ÃvbÇÁ
,8C
±yzfQ
¼
X!RL
ÃÇÁ[j!(6
?/:
j!(
?/:
j!(
1R M:`Q\ 1` M:``Y
1X M:`NN 1RM M:`LN
1Q M:N`R 1RR M:`R_
1_ M:`L_ 1RX M:`Y_
1L M:`X_ 1RQ M:`NY
1Y M:``Y 1R_ M:`LL
1\ M:`\` 1RL M:`LQ
1N M:`\`
$
‡,
µ$ÏÛ[“Ä0Œ¼.
!
]²ƒ„[
_
¢µ
-QR\-
{
QY
ï{
Y
—
XMRR
÷
Q
´
!!!!!! ! ! ! ! ! !!!! ! ! ! !
U/&fQY! ;004(!Y
=$%G#! XMRR
$Ï۔•
!LMh
”•
!
Š•
!LMh
Š•r
!

LMh
Š•µ$[®>}QȐ(„‘
!
ÈVW„£
!

$ÏÛ¶·
LMh
Š•

CŸÛ
#
Ê=
X
¢YZµ$
…©[“Ä0Œ¼.
!X
¢µ$…©µ$é[jÐ
!
“½hŸÛÝE„ym
!
>µ$…©¶·ŸÛ

C
YZ[µ$9’
RL!QM!_L!YM I)
[“Ä0Œ¼.
QM I)
¾¿9’-[µ$é[s£|>
!
>¶·Ÿ
Û9’ê
QM I)
²/ԓ
LMh
Š•ŸÛ
QM
I)
êµ$…©

£¦§6ѓĉ”•
<
_
#
Š.
<
_
#
”•
<
ÄB
_ъ.
<
ÄB_
_
=ÊjHå
!
0Œ€TғŠ
.
<
ÄB_=ÊjHå
!
¿È[6ˆ(„ß
!
nsp
—d
!
讕zfQ[6
!
Ã#~ßғŠ.
<
ÄB_HåEê=ÊjHå

£¦§Í“
b$2(%0
[
8T>
”&àîËã®+
OÛzpq
!
]
XQM )I
Ûz¬
!
}Qfspt4„
,
!
±yȱ\„¡
!
}QÈnj„ŸO
!
œÄƒ„
¾
!
¶·
XQM )I
Eê꣦§[”&Ûz

Ÿ¡éJj}Q©
$,8C%
ғ
RfN
!
I

K}QÚÞÂ
!
³h££µ¡Úé
!
ÍÇÁr[Ì[
]
` I)
~6ˆÚê*i
&
$®N•Úé¡
!,8C
²×[}QÚz÷f
!
£¦§Ò“[
.11 AQ
Úä|
¢
RM GI
[}QÚ
!
)bä
,8C
6ˆN(R[²
|k&ÈÃ

$
Ž
%
R(!
r­ÇÒ
:

1(:XMRM, `Y:
X(!
ª]
!
Ââ5
!
•)`
!
‡
:
vbieb
.8C
zfQƒ„
9(:
r­Ç_¥¦
! XMM\! _X$N%, LNR:
Q(!
6g
!
7Nþ
!
8PŽ
!
‡
:
vbÎt
.8C
zfQ[Ô·À
½ƒ„
9(:
r­rÇ¥¦
! XMM\! QX$RX%, RRYR:
_(!
ô‹
!
ãæ.
!
v9
!
‡
:.8C
i
,8C
}QâsMQ…©ƒ
„
9(:
6ç§Ü
! XMMN! X\$_%, LY:
L(!
ÂgÎ
!

!
ô£:
!
‡
:
Ÿ¡éJj}Q
$,8C%
“•|’
ÇÁ_ϝÚ6zfQƒ„
9(:
šø_ùÓ
444

ÇTô^
! XMM\! `$Y%, _Y:
9P;2LE/G/LDAG0KD0LLEGB./DBUG/NE0LNGBM01ABMP/ABC0/A:/H0Q 61O/
d.>?@e
R
! b>?@d#()a#/)*
X
! +;>Ob(
X
! d.>?@C$)*^
R
! C;e)*
Q
! 7;D$0#4)
Q
! 9;>c)*
R
!
$RfA:..=.&4+#@%!%.,#=*:%,<Xf7%#,89 /#,%., 2:#+;#<9!%#=*.f! 5!@f! 5%#,?9,8#,8 XXXMMR! *:%,#&
QfA:..=.&2:#+;#?!A:<,?#,8 2:#+;#<9!%#=U,%-<+%!?! A:<,?#,8 RRMMRY! *:%,#%
6OKDG/LD(8OWALD0SA, A/5(E(&/V $) ,8CI(2#/5 /65(2(%I))*2#(G#$%$G2(%02GG#%/I$2/*%$V#GV%/6&(0/68$(/)$(3$<
5K>&P$6/%^ 4$&2BG/)2%/&f>ADEBH, A#(,8CG#$%$G2(%02GG#%/I$2/*%$V#GV%/6&(0/6662(() P$2G#(0/68$(/)$(3$5K>&P$F(%(
5(2(%I)(5 /) $) .11 AQ /&4I) $XfR IIgRMM II! RfN
!
I% (&42(5 F2# 2#(I/P&(V#$0(0/6F$2(%G/)2$))*MfMLh V#/0V#/%G
$G5 $)5 $G(2/)2%&() *%$5()2I/5(fA#(5(2(G2/) F$E(&()*2# F$00(2$2XQM )If:AKI1D,A#(G/II/) I/5(/62#(,8CG#$%$G2(%<
02GG#%/I$2/*%$V#GV%/6&(F$00(24VfA#(%(F(%(RL G/II/) V($W0!6E(/6F#G# F(%(5()26(5!$)5 2#(0I&$%5(*%((0/62#(66<
2(() 0$IV&(02/2#(G/II/) I/5(F(%(P(2F(() MfN`R $)5 Mf``Yf2BCL1IK0BC, A#(I(2#/5 F$02I(<0$E)*$)5 G$) P(40(5 6/%2#(
^4$&2BG/)2%/&/68$(/)$(3$5K>&P$f
XAF ZBGHK(!8$(/)$(3$5K>&P$& G#$%$G2(%02GG#%/I$2/*%$V#GV%/6&(& ,8C
HB0,!+ %`#)RLWL..#+!!+!$
$
‚ƒ$Q
!
Š‹Œ
%
-_R\-
{
QY
ï{
Y
—
XMRR
÷
Q
´
!!!!!! ! ! ! ! ! !!!! ! ! ! !
U/&fQY! ;004(!Y
=$%G#! XMRR