免费文献传递   相关文献

Rapid determination of puerarin in Xiaoke pill powder by near-infrared spectroscopy

近红外光谱法快速测定消渴丸药粉中葛根素含量



全 文 :–P®KQ©RN&ÔSTUÇVrWìû\·
Zrs
!
#
)t
#
u±#
#
Ôv
#
ô]c
!
ùR5îHKNOPQ
#
ùR
LRMLQM
$
”;
%!

&
ғ–P®KQ©CSTUÇVrWìû\·îËRN&Ô

–—
&

.8C
6aEê’2
!
ғ–
P®¤ÅIKQùÓÒ°STUÇV[–P®KQ
!
0ÄD~8ýP©BCWìû\·[RN&ԅ©
!
>C|ï®>îË
‰\·Ë&

˜™
&
BC[WìûÇ»Xâ
R
X
!3=1-U!38T
6Ñê
Mf`NM R!MfRQR!\fM`
CË&°®>Ë&—ŒjCDE
ê
QfXh
˜š
&
à…©,/
#
RN
#
ym
!
*EêSTUr’ä>[·”&Ѧ9]p[·@Ü[…©

$
›œ
%!
–P®KQ©
&
STU
&
Wìû
$
8…$f
%!XMRRMXXNMML
$
†‡Eq
%!
­æ
.
k£‹Ç=Ü
/
øùk£­u
$XMM`d+M`QMN<
MMQ%
$
ˆ€>‰
%!
!
ËQR
!
¡¢N?Ä
!A(&,$MXM%QXXRNNYY!-04P%4]XRG):G/I
!!
STUê
XMRM
ր
*
r­ÇÒ
+
JS>¢
!
ä
NWì
#

#
¨
#
ÅJ£T‡
N
èÇÙÚ[r,
Çl…ÜÛ
!
yèUŸŒà
#
V(ãÎ[àé
!
ÛF
_9W\“•‘Î
#
‘X
#
‘J
#
SY
#
ÿZ-P
#
[
E
#
\ög(à=]²>[ST•
!
L
X
â7X•Ê
_¢ÆëF
R(

WìûEêSTU[·@Ü[|k&À
!
ɓ[\·&ԅ©ê¡éJj}Q©
!
ì#©Ž
]69’z
#
60Œ^¾
#
Y®•]ãä ?r
¦96‡D

Ã#
!
_׃„|¢rǏÚ
6\·[RN&ԅ©
!
)Yúè䕵5STU
ãä ?[·@Ü_—
!
hnC rÇN8ùÓ
îjÑä>[·5¢yèk&T¦@ù

–P®KQùÓ
$?;3%
ä–÷;®N€Ë[|
¢‹âKQ6ùÓ
!
yèRN
#
¡é
#
-ö÷
#
‚%
`G¦9]p6‡“-
!
Ñ]ð8
#

#
`
^
#
úLJ‘¯°h9W\“
X(
?;3
©]rÇ
Á‡:ëÇÌ\·&ԅVb$‰|Ô[ƒ„Ú
Œ
!
ìl|ʪ\“•l…ÜÛãä ?r’ä>
[Wìû\·&Ô[4ø

£ƒ„X–P®KQ©
i^_/·_j0Ä
!
ғD~8ýP©BCÔ·
6Xâ
!
¦TCSTUÇVrWìû\·[RN
#
ym
#
,/&Ô
!
ª0ŒèÌ\“•STUãä ?
[¦9[·@Ü

!
ÁÂ
bCcFQ–P®KQß
!
ÐdÀÿBe[f
gh”&à
#
¤ÅIW6i
#
®>AM˜
#
®>jÑ
O8,1
^_/·_fs
$=8>
â
!

7%4W(%
˜

%&
¡éJj}Qß
$>*&()2RRMM
â
!

>*&()2
˜
%&
1“:—
$R[R
m
!+AXXM>
â
!

8%(G0$
˜
%
WìûC2>
$
r­Ç>ãÌÜ>”Ô²
!
Ã
f
RRM\LXSTUÇV
$_M
Ã
!
9-r|Ç
8è&˜
%&
”•
$
}QO
%&
ŸO_

#
…©
# !^
–P®KQÒ°
!
$
_M
ÃSTUÇV®>
!
:B
RM *!
?Ò`Ž®>jr
!
“À,OsîËO
®Ö¤¾
!
e(ꒃ
!
oN¢w
!
®>jAM…
šÒ°KQ

&®…š
,
W6i¤ÅI
!
pq4Æ
RX MMM m_ MMM GI
SR
!
6 [
N GI
SR
!
pq5(
Y_
5

:®>kl?®&Ô
Q
5
!
/R—ŒKQ
BCXâ
!_M
STUVo®>[–P®KQra
fÊf
R
f
R!_M
STUÇV[–P®KQf
-X\Y-
{
QY
ï{
Y
—
XMRR
÷
Q
´
!!!!!! ! ! ! ! ! !!!! ! ! ! !
U/&fQY! ;004(!Y
=$%G#! XMRR
# #^
STUÇVrWìû\·
.8C

!
}Q
âs
, b$2(%0
RN
}QÚ
$ _fY IIgRLM II! L
!
I%&
=Êj”•
<
_
$XLp\L%&
”&Ûz
XLM )I&
î
®·
RM
!
C&
=N
RfM IC-I)
SR
&
Ú¤
QL l
Aâ9’ԝ
!
ÈVWÔ·
!
®À©/R

W
ìû]
MfM`_ R mMf_\M L
!
*
iÈVWžß[p
‰H
!
Ê<…?
GZQ XNQFnQR LXX $+Z
Mf``` \%&
93(
#
dԝ
#
kl
31T
6Ñê
Mf`Nh! RfLh! RfRh!
¼.£©93(
#
dԝ
#
k
lŒ„ß
&
—ŒÊJ[ê
RMRfMh!31TRfRh
:®>—Ë&Ô
X
5
!
$—Œa
_M
ÃSTUÇ
V®>Wìû\·4Æê
\fY` mRRf_M I*-*
SR

# $^
Ô·Xâ[BC
!
X
_M
î>q¼6êÇ»
°ÑË&°
!
ªrÇ»°
QM
Ã
!
Ë&°
RM
Ã

Ç»
°®>“•Ç»Xâ[BC
!
Ë&°Y’iBX
!
“
•Xâ[§Æ

XÇ»°–P®KQi
.8C
6aj‰
¹
!

O8,1
Ô·6fsr

CKQËÖ¤
…©î˃„
!
>“^BX[KQ+’
!
ғD
~8ýP©
$8C1
©
%
Ñt¿§Æ©
$G%/002/)%
BCÔ·Ç»Xâ
!
>¾ÔH(
$R
X
% #
t
¿§ÆÇ»À,DE
$3=1-U%
Ñt¿§Æj
C6.E
$38T%
‡’(EêXâi[AD
À

ªr
!R
X
G–•
R#3=1-U
G8
!
¼.
Xâ01GĤ
!38T

!
¼.Xâ[Ë&
iÑœiPGò
Q(

$

$ !^
KQËÖ¤…©¶·
!
–P®KQNw\®
>[nûnj®
!
œw\‰ªÇ-‰njÑtÛ
!
ü
1tÛ
#
®>¢wÑ¥+K‡

Ã#
!
]BCXâ
9
!
SNKQ()-‰njÑtÛF!6‰ŠÑ
–&
_(

£¦§C‘¢KQËÖ¤…©îˉƒ
„
!
ʼ
R!

3=1-U!R
X
!38T
EêADÀ
!
“¶K~Ô[ËÖ¤…©

0Œw½
!
|uÀ(0đ;+IÇ»ê~Ô
[KQËÖ¤…©

À(KQ*èéQSNspÑ
ªÇ¢w[6ï
!
6 krÈ
!
µ¡6 [ÑvO
(

‘;+IÇ»*SNùÿwF£8
#
¼V+
IGK?F^C¤ÅIKQ[°±
L(

®>[
|uÀ(KQfÊf
X
$ #^
Ûz+’[¶·
!
]
?;3

8C1
…©BX
r
!
$åæ-)ê
8C1
yè„ò[f6ïiP
!
*
!!
¼
R!
YZKQËÖ¤…©CXâi[°±
KQËÖ¤…©
3=1-U
R
X
38T
-KQËÖ¤
M:X_R M:`_X R _:N‘;+IÇ»
$=1% M:R\_ M:`Y_ _ L:Q
À,»îF·FQ
$1?U% M:RLR M:`\Q ` Y:R`
ýuÀ(
R%
M:R_\ M:`\L Y:QX
|uÀ(
R%
n
x·<|^
M:RLL M:`\X _ Y:MQ
|uÀ(
R%
n
‘;+IÇ»
M:RQL M:`NM R Y:`_
!!
?
,
R%
À(©Í“
)/%0`
-—y

f
X!
®>[|uÀ(KQf
OÛz’i‘;Ç»Xâ[BC

q2C
8C1
©[ó҃„Ñ\“
!
m ±Ô…©z¶Ûz+
’è*ihË&iPò
#
dïâß[Ô·Ç»

Q(

YZÛz+’CXâi[°±Ê¼
X!
0Äfs[Ûz+’“^ài
!
/Ô¶·BX
[Ûz+’ê
\ LMLf` mL __YfX! _ YMLf_ m
_ X_XfN GI
SR

¼
X!
YZÛz+’CXâi[°±
BXÛz+’
[GI
SR
3=1-U
R
X
38T
RR `N\:` m_ M`_:X M:XM_ M:`YY ` Y:RN
\ LML:` m_ M`_:X M:R_` M:`\\ _ Y:\\ LML:` mL __Y:X!_ YML:_ m_ X_X:N M:RQR M:`NM R \:M`
$ $^
‚Ó([¶·
!
ғ
8C1
©BCXâ
9
!
²¶[‚Ó(CXâË&iPè‚É£[
°±

‚Ó(Ög
!
KQr|íè“[njl
|&w\hÀ>XâË&iP{Ô
&
‚Ó( 
‘
!
EKT ÌÄTìh°±ª0Œ
Y(

£¦§
ғt¿§Æ©“ÄYZ‚Ó(CXâ
3=<
1-U
a[°±Êf
Q!
£¦§Ò“[~ԂÓ

N
-Q\Y-
{
QY
ï{
Y
—
XMRR
÷
Q
´
!!!!!! ! ! ! ! ! !!!! ! ! ! !
U/&fQY! ;004(!Y
=$%G#! XMRR
fQ!
‚Ó(f
$ %^
Xâ[BCÑt¿§Æ
!
–P®KQÍ |
uÀ(
n
‘;+Iǻ֤¾
!
]
\ LMLf` m
L __YfX!_ YMLf_ m_ X_XfN GI
SR
Ö
!
¶·
N
‚Ú
6BC‰WìûÔ·Ç»Xâ

àXâ
R
X
ê
Mf`NM R!3=1-U
ê
MfRQR!38T
ê
\fM`!
>CàX
âîˉt¿§Æ
!
ªjzê
R
®>
!
0ŒÊ¼
Q QM
ÃÇ»°®>t¿§Æ—ŒjCDEê
Xf`h!
¼.Xâi„ß

$ &^
ғË&°CÇ»Xâî˧Æ
!
“Ç»°B
C[WìûÔ·6Xâ
!
CË&°r[
RM
î>
îËÔ·6
!
h[Ë&å/0ŒÊ¼
_
Ë&0
Œ~£jCDEê
LfRh!
~8jCDEê
MfYLh!
—ŒjCDEê
QfXh!
Xâ[Ë&錞ß

¼
Q!
WìûÔ·Ç»Xât¿§Æç§
®>Ãf
*¦a
[I*-*
SR
Ë&a
[I*-*
SR
DE
[I*-*
SR
jCDE
[h
®>Ãf
*¦a
[I*-*
SR
Ë&a
[I*-*
SR
DE
[I*-*
SR
jCDE
[h
=MMX_N RM:L\ RM:YY SM:M`M M:NL =MRX`R RM:QM RM:\X SM:_XM _:R
=MMXLM RM:\M RM:NX SM:RXM R:R =MRX`_ RM:Q` `:NX M:L\X L:L
=MMXLX RM:_M `:`X M:_NQ _:Y =MRQMM RM:_` RM:\M SM:XRM X:M
=MMXLQ RM:\N RR:R` SM:_RM Q:N =MRQMQ RM:_Q RM:\X SM:X`M X:N
=MMXL\ RM:LL RM:X\ M:XNM X:\ =MRQM_ RM:LL RM:\X SM:R\M R:Y
=MMXYQ N:NL N:\_ M:RRQ R:Q =MRQMY RM:QY RM:L` SM:XQM X:X
=MMXY_ N:\Y N:Y_ M:RX_ R:_ =MRQM\ RM:LL RM:`\ SM:_XM _:M
=MMXYL `:QY `:RN M:RNM R:` =MRQRR RM:`N RM:Y` M:X`M X:Y
=MMXYY \:Y` \:X_ M:__N L:N =MRQRX RR:_M RR:XN M:RXM R:R
=MMXY\ N:XX N:LQ SM:QRQ Q:N =MRQR_ RM:_M RM:Y_ SM:X_M X:Q
=MMXYN N:R\ N:XN SM:RM` R:Q =MRQRL RM:_` RM:Q_ M:RLM R:_
=MRXQR RM:LX RM:`_ SM:_XM _:M =MRQRY RM:NL RM:\R M:R_M R:Q
=MRXN\ RM:X_ RM:\L SM:LRM L:M =MRQR\ RM:\` RM:YR M:RNM R:=MRXNN `:_` `:QR M:RN_ R:` =MRQRN RR:MN RM:LY M:LXM _:=MRX`M RM:QX RM:`R SM:L`M L:\ =MRQXM RR:ML RM:LL M:LMM _:L
¼
_!
WìûÔ·Ç»XâË&0Œå/
®>Ãf
*¦a
[I*-*
SR
Ë&a
[I*-*
SR
DE
[I*-*
SR
jCDE
[h
—ŒjCDE
[h
=MMX__ RM:RR RM:L_ SM:_QM _:Q
=MMX_\ `:RX `:_X SM:QMM Q:Q
=MMXLR RM:RL `:`X M:XQQ X:Q
=MMXY` RM:\N RR:R` SM:_RM Q:N
=MMX\R N:Y_ N:`\ SM:QQM Q:N
=MMX\X `:X` `:RN M:RRM R:X
=MRXN` RM:\R RM:Y_ M:M\M M:YL
=MRX`Q RM:__ RM:MN M:QYM Q:_
=MRX`L RR:MM RM:__ M:LYM L:R
=MRQRQ RM:R_ RM:LQ SM:Q`M Q:N
Q:X
%
0,
£¦§m –P®KQ©i^_/·_ùÓj

!
ғD~8ýP©BC‰STUãä ?[
r’ä>ÑÔÇVrWìû\·[6…©
!

¼.
!
à…©,/
#
ym
#
RN
#
-ö÷
!
*¦TCS
TUÇVrWìû\·[RN
#
ym
#
,/&Ô
!
ª
-_\Y-
{
QY
ï{
Y
—
XMRR
÷
Q
´
!!!!!! ! ! ! ! ! !!!! ! ! ! !
U/&fQY! ;004(!Y
=$%G#! XMRR
0ŒèÌ\“•STUãä ?[¦9[·@Ü

$
Ž
%
R(!
r­ÇÒ
:

1(:XMRM,RM_R:
X(!
¡âò
!
4š|
:
Tô–P®KQ6ùÓ[ȤG\“
9(:
6ßà
!XMMX!$Q%, `:
Q(!
}~
!
€|
!
‚8C
:
–P®KQßà
=(:
üý
,
^_N
8Kĺ
! XMRM:
_(!
‚8C
!
€|
!
}~
:
–P®6rKQËÖ¤GÛz¶
·…©îËi\“
9(:
^_îË
!XMM_!RY$_%,LXN:
L(!
}~
:
Tô–P®KQ6ùÓ
=(:
üý
,
r­`^KÄ
º
! XMM\:
Y(!
2ƒ„
:
–P®KQ6s¨i\“
=(:
üý
,
r­…N8
Kĺ
! XMML:
:/N0HHADAG.0C/D0BCBMNIAG/G0C0CY0/BVAN01NBZHAG
OF CA/G-0CMG/GAHKNALDGBKLBNF
1,7%4
!
! c-7)! @-?@#4)K$)! 1.;=()*! b,#$)*#$
$S9#,8Q:.9 P:.,8?%2:#+;#<9!%#=*.6! 5!@6! S9#,8Q:.9 LRMLQM! *:%,#%
6OKDG/LD(8OWALD0SA, A/5(2(%I)(2#(G/)2()2/6V4(%$%) ) +$/W(V&V/F5(%%$V5&BPB)($%<)6%$%(5 0V(G2%/0G/VB:
>ADEBH, ?($%<)6%$%(5 5640(%(6&(G2$)G(0V(G2%/0G/VB2(G#)/&/*BF$040(5 2/G/&(G2?;30V(G2%$/6+$/W(V&0V/F5(%:b2# .8C
$)$&B00E$&4(0$0%(6(%()G(! 2#(6$025(2(%I)$2/) I(2#/5 /6V4(%$%) F$0(02$P&0#(5 F2# V$%2$&&($020^4$%(0$8C1%::AKI1D, A#(
3
X
! 3=1-U$)5 38T/62#(G$&P%$2/) I/5(&6/%V4(%$%) F(%(Mf`NM R! MfRQR $)5 \fM`:A#($E(%$*(%(&$2E(5(E$2/) /62#(
V%(5G$2/) 0(2F$0QfXh:2BCL1IK0BC, A#(I(2#/5 0$GG4%$2(! 6$02$)5 0IV&(! F#G# G/4&5 P(*()(%$&a(5 2/2#(/)<&)(^ 4$&2B
G/)2%/&/6+$/W(V&V/F5(%V%/54G2/):
XAF ZBGHK(!)($%<)6%$%(5 0V(G2%/0G/VB& +$/W(V&& V4(%$%)
HB0,!+ %`#)RLWL..#+!!++$
$
‚ƒ$Q
!
Š‹Œ
%
-L\Y-
{
QY
ï{
Y
—
XMRR
÷
Q
´
!!!!!! ! ! ! ! ! !!!! ! ! ! !
U/&fQY! ;004(!Y
=$%G#! XMRR