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期 刊 ：中国中药杂志 1999年 24卷 01期 页码：14.

关键词：雷公藤；雷酚内酯；薄层扫描法；

Keywords:Leigongteng, triptophenolide, TLCS,

摘 要 ：目的：建立雷公藤中雷酚内酯含量测定的方法。方法：采用薄层扫描法，样品上柱纯化，以氯仿 乙醚（２∶１）展开，Ｋｅｄｄｌｅ试剂显色，扫描，外标两点法计算。结果：线性范围为２．１～１０．５μｇ，ｒ＝０．９９８。结论：本法可作为雷公藤质量控制的方法。

Abstract:Objective:To establish a method for the determination of triptophenolide in Chinese herb Leigongteng(Tripterygium wilfordii Hook.f.).Method:TLCS was used.The sample was purified with a column and developed upwardly with CHCl 3 EtOEt(2∶1),sprayed with Keddle testing solution and scanned.The content was calculated with external two point method.Result:The linear range was 2.1μg～10.5μg,r=0.998.Conclusion:The method is proper for the quality control of Leigongteng.

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