免费文献传递   相关文献

Simultanenous determination of contents of four nitrogenous compounds in Pinellia peda-tisecta by HPLC

HPLC同时测定掌叶半夏中四种含氮化合物的含量



全 文 :.8C
Z7%ԗ˜™šr– Z›\ÄÌ[Z·
þùe
P#O
#
¯‚B
P#W
#

P#W
!
#
$…n
&
#
.±
^
#

^
!Ph
óï8HKA¯ 8K¯J
#
óï
PMMPMW%
Wh
8KéG©ÊAH5(<ëjLM8!
#
óï
PMMPMW%
Oh
×¹IæðI¯LMJ
#
üó ×¹I
MLMM^P%
^h
óïæðOô#JãK
#
óï
PMMPMW
$
‚;
%!

&
›#ésj{m”Z7%ԗ˜™šr¡>~{
#
p¾¢ì
#
¾£¤Ñ
X<
­£¤
^
 Z›\ÄÌ[Z·

•–
.

R$I/)0&<
PN
{m”
$^hX IIiPLM II! L
!
I%&
“e
<

<
ƒ“Uf\g
!
1L
PhM IC/I)
QP
&
”@
WL j&
W%Á
x
WL^ )I
—˜
.
¡>~{]
MhW gPhM
!
*$:YMh___ X%!
p¾¢ì]
WhX gPO
!
*$:YMh___ N%!
¾£¤]
MhLL gWh[L
!
*$:Y
Mh___ _%!X<
­£¤]
MhXL gOhWL
!
*$:YMh___ N%
n›‰Fo!
&
¡>~{@ŒÈHs
PMMhXm!31RWh^m$(YX%&
p¾¢ì@
ŒÈHs
__hN_m!31RMhWMm$(YX%&
¾£¤@ŒÈHs
PMMhLOm!31RPhPm$( YX%&X<
­£¤@ŒÈHs
PMMhMm!31R
Ph^m$(YX%
—™
.O
ÃGF%Ô0•¼.
!
4…”yÉ
#
+/
!
*›—˜™šr
^
 Z›\ÄÌ[Z·%Ô

$
ƒ„…
%!
—˜™š
&
Z›\ÄÌ
&
#ésj{m
$
8†$f
%!WMPMMNOMMMW
$
‰€>Š
%!
!
þ7O
!
Ž/
!
z{ãMä
!A(&. $MPM% N^[ONOO^!
-$
>Šš›
%!
g-t
!
z{ã
!
‚&±×rǙ¬[—i\›ƒ
„
!-!!
—˜™š
?(1.7 *1+7B!916!7 1G#/2
N8ýV
öÉÌ
!
«M¥—ýV
!
Õ|[Üëï#ÐÇ
!
N
rÇ8ýV[‚&;¬g|
!
wè=bÔ¦
#
\›2
0[Þg
P(

—˜™š‚&ZèãÌ{¨\ÄÌ
!
¡¨\ÄÌ
!
ü¼¨\ÄÌ
!
6虠•s@¨
#

Ž¨GX·8—‡Ú6
W(

RôÇ¥ƒ„¼.
!
¡>~{wèIQ[m‚‡
#
ðQI‡E›
O(

p
¾¢ìNÄÚms‚uÇ̧›p¡
#
ªŽp¡G
j‰ÇÌ[‰Šršþ
!
`NÄÚm‚‡
#
mu¼
#
<
p¡[³˜ÈÂ
^(
&
¾£¤[¡@曝¿ È
Yû^´ãä
#
’r¼
#
m‚‡ÇÑmŒë¾Ç‡“
³[tab»eª
!
`›O›Öab»eª
&X<
­
£¤Ni&[*@*¡

¤7]‘j‰7«[s
©_
!
¬›#ésj{mõ-Z7%ԗ˜™š
ï#r– Z›\ÄÌZ·[…”

!
ÁÂ
>*&()2PPMM
#ésj{mFã
!D` (
c ÙÁó\ß
$
¾óS Ùßàè#–$
%!1$%<
2/%/407AWL1
â
PZPM
.N6‹8@
$
øùå™
¬;ßàè#–$
%
ŒŽ
#
“e
$J0#(%
–$
!
{m
=
%&
¨©k=ì¸
&
ªÆçیê6‹=

§¨²›GF—˜™š Ü
WMM_
÷
W
²ø
Ìøò­ÇÁSH
!
>Ëøùr…Ç|]Ïìã
Ž/ÕÔ
!
ꗘ™š
?h*1+7B!916!7 1G#/2
 Ü
&

O
²tV89 Ü Éøùr…Ç|]ÇÉ
Q~
!PM
²ªª|>MK Ü
!

#
°Õ
!
EêG
F

¡>~{À+Før­ÇFãÌÜFWÔ
²
!
Ãfê
PPMNNOË
.8C
”W%ª=
__h[m&
p¾¢ì
#
¾£¤Ñ
X<
­£¤A“Fø8
}|…ãÌö÷–$
!
Ë
.8C
”W%ª=6Œ
ê
__h^m! __hWm! __hXm
#
…”i0•
# !^
{mïqGFã2››ç¨
!R$I/)0&<
PN
{m”
$ ^hX IIiWLM II!L
!
I% &
f\g
!
M gPM I)!
“ e
Lm g PMm!
¸
_^hNm g
N_hNm!
ƒ“U
MhWm&PM gWL I)!
“e
PM g
WLm!
¸
N_hNm g[^hNm!
ƒ“U
MhWm&
1L
PhM IC/I)
QP
&
”@
WLj&
W%Áx
WL^)I&
¦
_£{mïq
!
G#A“FñsÑoçFñs¿
PM
!
C
6ΔG
!
]A“FñsÑoçFñs{
m$wèjZA´7š
!
Ãd
P
# #^
A“Fñs[ÜÝ
!
93P#
^
 A“F
$
¡
>~{
#
p¾¢ì
#
¾£¤Ñ
X<
­£¤
%

!
›1
Êjá£Ú<6Œê
MhM^! MhLW! MhPP! MhPO
/^OOP/
{
OX
ï{
PM
•
WMPP
÷
L
²
!!!!!! ! ! ! ! ! !!!! ! ! ! !
S/&hOX! ;004(!PM
=$B! WMPP
!!
>:
—˜™š
&7:
CÄA“F
&Ph
¡>~{
&
Wh
p¾¢ì
&Oh
¾£¤
&^hX<
­£¤

d
P!
—˜™š
.8C
d
*/C
QP
[A“Fñs
!
ݛ

# $^
oçFñs[ÜÝ
!
93P#—˜™šG_
$
¡
XM

%W *

LM IC
·ír
!

LM IC
Œ
Ž
!
 Ù–«
OM I)!
X TX¡T
!
ݛ

# %^
n›‰F‘K
!
#¡>~{
#
p¾¢ì
#
¾£
¤Ñ
X<
­£¤A“Fñs
!
<6ΐ
MhM^! MhLW!
MhPP! MhPO */C
QP
!
]
# !^
u[{mïqª
!
6Œ9
3G#
L! PM! PL! WM! WL
!
C!
?Ðsj{mß
!
%
Ô¿{m$$TU

A“F·
$
!
*%
ê/À
!
{
m$$TUꎍÀîÉn›È9
!
0•Ã¼
P
¼
P!^
 A“F[È9…ôÑn›2Â
A“F È9…ô n›2Â
Z
!
* :
P OYW[ _NLSQW M[OAM M:W gP:M M:___ X
W OYPN OPLSQW PXOA^ W:X gPO M:___ N
O OYW[ ^PXSQO ON[AP M:LL gW:[L M:___ _
^ OYWW _PXSQO PXXA[ M:XL gO:WL M:___ N
# &^
93‘K
!
#—˜™šÇÁG_
!
’
# $^
u
ª…”
!
ÜÝoçFñs

]
# !^
u[{mïqª
!
93G#oçFñs
PM
!
C!
¯ÆîG
X
5
!
%Ô¡
>~{
#
p¾¢ì
#
¾£¤Ñ
X<
­£¤{m$$T
U[
31R
6ΐ
PhWm!PhMm!PhWm!PhNm
¼.
ßà[93o!

# ^
ŸÔ›‘K
!
#
# &^
uªoçFñs
!
6Œ
Üݾ
M! W! ^! X! N! PW! W^ #
îG
!
%Ô¡>~
{
#
p¾¢ì
#
¾£¤Ñ
X<
­£¤{m$$TU
!
.
P
31R
6ΐ
Mh__m! WhWm! PhXm!Ph_m
¼.
GF]
W^ #
~s¤ŸÔ

# (^
ij›‘K
!
#Z|ט™šÇÁG_
!
9
3PÔ
X
t
!
’
# $^
uª…”
!
ÜÝoçFñs
!
@
É%Ô
!
.P¡>~{@ŒZ·ê
MhPXm $31R
PhOm%!
p¾¢ì@ŒZ·ê
MhMNm$31RWhOm%!
¾£¤@ŒZ·ê
MhMLm$31RMhXm%!X<
­£¤
[@ŒZ·ê
MhP^m$31RPhOm%
¼.4…”i
j›o!

# )^
aGÈHs‘K
!
P#ÏíZ·[—˜™š
X
t
!
7t
P *!
93PÔ
!
6Œ93aС>~{
#
p¾¢ì
#
¾£¤Ñ
X<
­£¤A“F2·
!
a1Ê
j Ùñl
!
;­±[
!
ˆ‘
!
X TX¡T
!
îG

!
.PÈHs

0•Ã¼
W gL
¼
W!
¡>~{aGÈHs
$(YW%
ÇÁ·
Z*
¡>~{
ZI*
aз
ZI*
%&·
ZI*
ÈHs
Zm
@Œ_
Zm
31R
Zm
M:___ N P:L__ [ P:L_M M O:WOM M PMW:L
M:__N [ P:L_[ _ P:L_M M O:WWM M PMW:M
P:MMP X P:XMW X P:L_M M O:PLM M _[:OW PMM:X W:^
P:MMO ^ P:XML ^ P:L_M M O:PXM M _[:[[
P:MML L P:XMN N P:L_M M O:W^M M PMW:X
M:___ P P:L_N X P:L_M M O:WPM M PMP:^
¼
O!
p¾¢ìaGÈHs
$(YW%
ÇÁ·
Z*
p¾¢ì
ZI*
aз
ZI*
%&·
ZI*
ÈHs
Zm
@Œ_
Zm
31R
Zm
P:MPN O M:NP^ X M:NPM M P:XWP ^ __:XM
P:MOO P M:NWX L M:NPM M P:XOX [ PMM:M
P:M^^ P M:NOL O M:NPM M P:X^L _ PMM:P __:N_ M:WM
M:___ [ M:[__ N M:NPM M P:XM[ P __:X[
M:___ L M:[__ X M:NPM M P:XM_ L __:__
P:MMW [ M:NMW W M:NPM M P:XPW M __:_N
¼
^!
¾£¤aGÈHs
$(YW%
ÇÁ·
Z*
¾£¤
ZI*
aз
ZI*
%&·
ZI*
ÈHs
Zm
@Œ_
Zm
31R
Zm
P:M[^ L M:LO[ O M:LWM M P:MLN N PMM:O
P:PWN [ M:LX^ ^ M:LWM M P:M_L ^ PMW:P
P:M_P ^ M:L^L [ M:LWM M P:MXX P PMM:P PMM:L P:P
M:___ N M:^__ _ M:LWM M P:MPL _ __:WO
M:__N L M:^__ O M:LWM M P:MPN [ __:NN
P:MWL [ M:LPW _ M:LWM M P:M^P W PMP:X
/LOOP/
{
OX
ï{
PM
•
WMPP
÷
L
²
!!!!!! ! ! ! ! ! !!!! ! ! ! !
S/&hOX! ;004(!PM
=$B! WMPP
¼L! X<
­£¤aGÈHs
$(YW%
ÇÁ·
Z*
X<
­£¤
ZI*
aз
ZI*
%&·
ZI*
ÈHs
Zm
@Œ_
Zm
31R
Zm
P:MM[ L P:^PM L P:^PM M W:NWP P PMM:M
P:MML O P:^M[ ^ P:^PM M W:NP_ _ PMM:W
P:MPL X P:^WP N P:^PM M W:NX_ L PMW:[ PMM:M P:^
M:___ ^ P:O__ W P:^PM M W:[__ [ __:OO
M:___ N P:O__ [ P:^PM M W:[_P L _N:[P
M:___ M P:O_N X P:^PM M W:[_X N __:PX
# *^
GFZ·%Ô
!
93P#Z5DH[
O
×
˜™š¿
O
t
!
’
# $^
uª…”ÜÝoçFñs
!
]
# !^
u{mïqªîÉ%Ô

®À”.P¿Ú6
[Z·

0•Ã¼
X
¼
X!
—˜™šGF[Z·
$(YO% m
Ã5¡>~{
31R
p¾¢ì
31R
¾£¤
31RX<
­£¤
31R
P M:P[ M:[ M:MN W:P M:MX P:N M:PX P:_
W M:P_ W:M M:PM P:P M:ML P:X M:PL W:O
O M:PL W:W M:PM P:O M:ML W:M M:PO P:N
$
0•i†,
稑KŒŽ
<
¸
#
“e
<
¸
#
ŒŽ
<
¡@¸
G“e
<
¸
<
ƒ“UþF

0•¼.
!
]“e
<
¸
<
ƒ
“U1ÊjþFr
!^
 Ú664o!
!
‡,Õ
½
!
›´µ41ÊjþF

§¨0•¼.
!

7õ-[{mïqª
!
*Z7%ԗ˜™šÇÁ
r
^
 Z›\ÄÌ[Z·
!
²%Ú6{m$iª
ÆÚ664o!
!
…”yÉTL
!
0•+/*+
!
*›ªY·cÜ

$
‹ŒŽ
%
P(!
»Š²
!
»¤÷
!
þ„t
!
‡
:
—˜™šƒ„¢´
9(:
r…Ç

! WMM^! WP$P%.PX
W(!
µ¬
!
(Ù­
!
»Ö
!
‡
:PM
 Ç›8ýV[\]Ú66‹
9(:
_&…ö|]]1
! P_N_! PX$O%.WMO:
O(!
8ˆó
!
=G
!
þ]®
!
‡
:
¡>~{[ ”%ÔGÇôÊN]
ƒ„
9(:
Ç]]1
!WMMO!ON$^%.W[_h
^(!
¯*é
!
ԙ°
:
®”ÄÚp¡
9(:
r­…ÇNþ£¤
!
P__L!WX[$_%.^W^:
=0.I1D/CACBIKHADAG.0C/D0BCBLTBCDACDKBLLBIGC0DGBUACBIKTB.MBICHK
0C>#,)0 %,&0?1/,410 NF 3O;2
+,CH4)
P!O
! c-;1#()*&
P!W
! c>?@c()]4$)
P!W
! @>T+4(B$)
P
! c>?@94)B)*
^
! C;C)
^
$Ph2,(191#1+6(12).131! M1D(3 E(F1:9!-)82,(191#1+6(1! M1D(3 PMMPMW! 2,(7&
Wh<(3(11:(3 %1917:6, 21(!1:)8$))+ 53:6/.!/:7.?:76!618):2,(1912:/+1P:/39! #(9!:-)8
<+/67!)(! M1D(3 PMMPMW! 2,(7&
Oh&,D7J,/7(3 567+10-)853:6/.!/:17(+ I):19!:-&61(619! &,D7J,/7(3 MLMM^P! 2,(7&
^hM1D(3 53:6/.!/:7.@16,().)3-6NKDG/TD(8N]ATD0RA. A/5(E(&/U $.8CI(2#/5 6/%2#(]4$)22$2E(5(2(%I)$2/) /66/4%)2%/*()/40G/IU/4)50) ?(1.7
*1+7B!916!7h>ADEBH. A#(5(2(%I)$2/) F$0G$%(5 /42/) R$I/)0&!
I% (&42(5 F2# $G(2/)2%&(<
F$2(%<2%(2#B&$I)() *%$5()2(&42/) $G(2/)2%&(QP
$)5 5(2(G<
2/) F$E(&()*2# $0WL^ )Ih:AKI1D.A#(&)($%%$)*(0/62%*/)(&)(!2#BI)(!$I5/U4%)($)5 #BU/K$)2#)(F(%(MhW gPhM
!
*$:Y
Mh___ X%! WhX!
*$:YMh___ N%! MhLL!
*$:YMh___ _%! MhXL!
*$:YMh___ N%! %(0U(G2E(&BhA#($E(%$*(%(G/E<
(%(0/62%*/)(&)(! 2#BI)(! $I5/U4%)($)5 #BU/K$)2#)(F(%(PMMhXm! __hN_m!PMMhLm $)5 PMMhMm %(0U(G2E(&B! $)5 2#(
31R/62#($d/E(6/4%G/IU/4)50F(%(Wh^m! MhWMm! PhPm! Ph^m! %(0U(G2E(&Bh2BCT1IK0BC. A#0I(2#/5 0%(&$d&(! $GG4%$2(
$)5 0U(G6Gh;2G$) d(40(5 6/%]4$&2BG/)2%/&/62#(24d(/6?A*1+7B!916!7h
aAF WBGHK(!?(1.7 *1+7B!916!7& )2%/*()/40G/IU/4)50& .8C
HB0.!+b%#)QT]T..#+!!!+!*
$
$Q
!
­Z®
%
/XOOP/
{
OX
ï{
PM
•
WMPP
÷
L
²
!!!!!! ! ! ! ! ! !!!! ! ! ! !
S/&hOX! ;004(!PM
=$B! WMPP