Abstract:This paper deals with the isolation of three new diterpenes: triptono-terpene, triptonoterpene methyl ether and triptolidenol from Tripterygium wilfordiiHook. F. Their structures are assigned as Ⅰ, Ⅱ, and Ⅲ, respectively by means of spectors-copic analyses (UV, IR, 1HNMR and MS), preparation of the derivative and chemicaltransformations.